Zeitschriftenaufsätze und Buchbeiträge

Sehr präzise Lufttemperaturmessung in der Meteorologie oder in klimatisierten Innenräumen sind herausfordernd, weil Strahlungseinflüsse und die Eigenerwärmung der Widerstandsthermometer teilweise erhebliche Störeinflüsse sind. In unserem Artikel betrachten wir eine spezielle Stromspeisung und weisen nach, dass diese die Eigenerwärmung auf unter ein Millikelvin reduzieren kann. Für einen typischen, für den Außeneinsatz in meteorologischen Wetterstationen geeigneten und üblichen Fühleraufbau erfolgen Simulationen der durch den gepulsten elektrischen Messstrom auftretenden statischen und dynamischen Eigenerwärmung. Der transiente Verlauf der Eigenerwärmung hängt stärker vom inneren Aufbau des Fühlers als vom Wärmeübergangskoeffizienten zur umgebenden ruhenden Luft ab. Die mittlere statische Eigenerwärmung aus einem stark vereinfachten Modell passt gut zum simulierten transienten Verlauf. Die Methode der Impulsstromspeisung hat sich durch die beschriebenen Simulationen als sehr effektiv zur Verringerung der Eigenerwärmung von Widerstandsthermometern erwiesen.

The majority of nanopositioning and nanomeasuring machines (NPMMs) are based on three independent linear movements in a Cartesian coordinate system. This in combination with the specific nature of sensors and tools limits the addressable part geometries. An enhancement of an NPMM is introduced by the implementation of rotational movements while keeping the precision in the nanometer range. For this purpose, a parameter-based dynamic evaluation system with quantifiable technological parameters has been set up and employed to identify and assess general solution concepts and adequate substructures. Evaluations taken show high potential for three linear movements of the object in combination with two angular movements of the tool. The influence of the additional rotation systems on the existing structure of NPMMs has been investigated further on. Test series on the repeatability of an NPMM enhanced by a chosen combination of a rotary stage and a goniometer setup are realized. As a result of these test series, the necessity of in situ position determination of the tool became very clear. The tool position is measured in situ in relation to a hemispherical reference mirror by three Fabry-Pérot interferometers. FEA optimization has been used to enhance the overall system structure with regard to reproducibility and long-term stability. Results have been experimentally investigated by use of a retroreflector as a tool and the various laser interferometers of the NPMM. The knowledge gained has been formed into general rules for the verification and optimization of design solutions for multiaxial nanopositioning machines.

A decrease of the temperature dependent coercive forces up to around 370 K is discovered in iron silicon alloys, both in quenched samples and in samples which were previously thermally treated to achieve the highest magnetic quality. Alloys of composition Fe-6 wt.% Si and Fe-3 wt.% Si are studied. This reduction in the coercive force is controlled by an increase in the mobility of the domain walls due to the increase in the dislocation's mobility enhanced by the movement of vacancies. It is worthwhile to mention that this reduction in coercive force is only present at these slightly elevated temperatures which are markedly smaller than the usual annealing temperatures for heat treatment of iron silicon alloys while it disappears again at room temperature. Neutron thermodiffraction, magnetic hysteresis loops tracer and mechanical spectroscopy are used as experimental techniques.

We investigate the free convection processes in the vicinity of a spherical 1 kg mass standard by two- and three-dimensional direct numerical simulations using a spectral element method. Our focus is on the determination and suppression of updraft forces in a high-precision mass comparator which are caused by temperature differences between mass standard and its environment in the millikelvin range - a source of systematic uncertainties in the high-precison mass determination. A two-dimensional model is presented first, which obtains a good agreement with previous laboratory measurements for the smaller temperature differences up to 15 mK. The influence of different boundary conditions and side lengths of the square domain is discussed for the mass standard positioned in the center of the chamber. The complexity is increased subsequently in configurations with additional built-ins for counter heating in form of planar plates or hemispherical shells above the mass standard. The latter ones lead to a full compensation of the updraft force. Three-dimensional simulations in a closed cubic chamber confirm the two-dimensional findings and additionally reveal complex secondary flow patterns in the vicinity of the mass standard. The reduction of the heat transfer due to the built-ins is also demonstrated by a comparison of the Nusselt numbers as a function of the Rayleigh number in the chosen parameter range. Our simulations suggest that such additional constructive measures can enhance the precision of the mass determination by suppression of free convection and related systematic uncertainties.

In this work, we review the viability and precision of the photon-momentum-based optical power measurement method that employs an amplification effect caused by a multi-reflected laser beam trapped in an optical cavity. Measuring the total momentum transfer of the absorbed and re-emitted photons from a highly reflective surface (reflection of the laser beam from an optical mirror) as a force provides the possibility of measuring the optical power with direct traceability to SI units. Trial measurements were performed at two different metrology laboratories: the laboratory for mass/force at the Technical University of Ilmenau, and the clean room laser radiometry laboratory at PTB, with a portable force measurement setup consisting of two electromagnetic force compensation balances. We compared the results of the optical power measurements performed with the force measurement setup, via the photon-momentum-based method, with those performed using a calibrated reference standard detector traceable to PTB's primary standard for optical power, the cryogenic radiometer. The comparison was carried out for an optical power range between 1 W and 10 W at a wavelength of 532 nm, which corresponds to a force of approximately 2000 nN at the upper limit, yielding approximately 2.3% relative standard uncertainty in the case of 33 reflections. Thus, conflating the high-precision force metrology technique at [my]N to nN levels with the optical setup required to achieve specular multi-reflection configuration of the laser beam, where a macroscopic optical cavity with ultra-high reflective mirrors (>99.995%) can adjustably be suspended from the force sensors, depending on required geometry of reflections, we show that the uncertainty of the optical power measurements upon further increase of the nominally applied optical power, the number of laser beam reflections, or the reflectivity coefficient of the mirrors can be markedly reduced.